000			05526cam a22004217a 4500
999			_c95806 _d95806
001			14169036
005			20260628184443.0
006			m o d
007			cr |n|||||||||
008			260629s2023 gw o 000 0 eng d
020			_a9783527348466
020			_a9783527831111 _q(electronic bk. : oBook)
020			_a9783527831104 _q(electronic bk.)
020			_a9783527831128 _q(electronic bk.)
041			_aeng
049			_aMAIN
050		4	_aQD75.4.C34 _bK67 2023
082	0	0	_223 _a543/.19
100	1		_aKościelniak, Paweł. _0http://id.loc.gov/authorities/names/n90690706
245	1	0	_aCalibration in analytical science : _bmethods and procedures / _cPaweł Kościelniak.
264		1	_aWeinheim, Germany : _bWiley-VCH, _c2023
300			_a1 online resource
336			_atext _btxt _2rdacontent
337			_acomputer _bc _2rdamedia
338			_aonline resource _bcr _2rdacarrier
504			_aIncludes bibliographical references and index.
505	0		_aCover -- Title Page -- Copyright -- Contents -- Preface -- Chapter 1 Calibration Fundamentals -- 1.1 Analytical Context -- 1.2 Principles of Analytical Calibration -- 1.3 Calibration Standards and Models -- 1.4 Calibration Procedures and Methods -- 1.5 Calibration in the Context of Measurement Errors -- 1.5.1 Uncontrolled Analytical Effects -- 1.5.2 Elimination and Compensation of Uncontrolled Effects -- 1.6 Calibration in Qualitative Analysis -- 1.7 Calibration in Quantitative Analysis -- 1.8 General Rules for Correct Calibration -- References -- Chapter 2 "Calibration-Free" Analysis
505	8		_a2.1 Novel Approach -- 2.2 Empirical Calibration -- 2.3 Theoretical Calibration -- 2.3.1 Fixed Models -- 2.3.2 Flexible Models -- References -- Chapter 3 Calibration Methods in Qualitative Analysis -- 3.1 Classification -- 3.2 External Calibration Methods -- 3.2.1 External Standard Method -- 3.2.2 Reference Sample Method -- 3.3 Internal Calibration Methods -- 3.3.1 Internal Standard Method -- 3.3.2 Indirect Method -- 3.4 Standard Addition Method -- References -- Chapter 4 Introduction to Empirical Calibration in Quantitative Analysis -- 4.1 Classification -- 4.2 Formulation of Model Functions
505	8		_a4.3 Examination of Interference Effect -- 4.4 Mathematical Modeling of Real Function -- References -- Chapter 5 Comparative Calibration Methods -- 5.1 External Calibration Methods -- 5.1.1 External Standard Method -- 5.1.1.1 Modified Procedures -- 5.1.2 Dilution Method -- 5.2 Internal Calibration Methods -- 5.2.1 Internal Standard Method -- 5.2.2 Indirect Method -- References -- Chapter 6 Additive Calibration Methods -- 6.1 Basic Aspects -- 6.2 Standard Addition Method -- 6.2.1 Extrapolative Variant -- 6.2.1.1 Modified Procedures -- 6.2.2 Interpolative Variants -- 6.2.3 Indicative Variant
505	8		_a6.3 Titration -- 6.4 Isotope Dilution Method -- 6.4.1 Radiometric Isotope Dilution -- 6.4.2 Isotope Dilution Mass Spectrometry -- 6.4.2.1 Modified Procedures -- References -- Chapter 7 Calibration in Nonequilibrium Conditions -- 7.1 Flow Injection Analysis -- 7.1.1 Manipulation Techniques -- 7.1.2 Gradient Technique -- 7.2 Kinetic Analysis -- References -- Chapter 8 Complex Calibration Approaches -- 8.1 Extrapolative Methods -- 8.1.1 Extrapolative Indirect Method -- 8.1.2 Extrapolative Internal Standard Method -- 8.1.3 Extrapolative Dilution Method -- 8.2 Mixed Methods -- 8.3 Combined Methods
505	8		_a8.3.1 Integrated Calibration Methods -- 8.3.1.1 Simple Integrated Method -- 8.3.1.2 Complementary Dilution Method -- 8.3.2 Generalized Calibration Strategy -- 8.3.2.1 Versatile Flow Injection Calibration Module -- 8.3.3 Standard Dilution Analysis -- References -- Chapter 9 Calibration Approaches for Detection and Examination of Interference Effects -- 9.1 Introduction -- 9.2 Simple Procedures for Detection and Examination of Interference Effects -- 9.3 Detection and Compensation of Additive Interference Effect -- 9.3.1 Interpolative Procedure -- 9.3.2 Extrapolative Procedure
520			_aUnivariate analytical calibration is a vital step in every chemical procedure that involves determining the identity or concentration of a particular substance. Depending on the type of instrument and measurement, analytical chemists need to follow different calibration strategies and protocols to ensure their instruments yield accurate readings. Calibration in Analytical Science systematically classifies and describes a wide range of calibration methods and procedures based on mathematical and empirical models for use in qualitative and quantitative analysis. Focusing on the chemical aspects of analytical calibration, this much-needed reference uses a set of equipment-independent terms and definitions that are easily transferable to the calibration strategies of any analytical process. The theoretical basis for calibration of each analytical mode is described and applied to common analytical tasks of increasing levels of difficulty and complexity. Throughout the book, the author illustrates how to combine different calibration approaches to create new calibration strategies with extended capabilities.
650		0	_aAnalytical chemistry. _0http://id.loc.gov/authorities/subjects/sh85023011
650		0	_aCalibration. _0http://id.loc.gov/authorities/subjects/sh85018860
655		0	_aElectronic books.
856	4	0	_uhttps://onlinelibrary.wiley.com/doi/book/10.1002/9783527831111 _yFull text is available at Wiley Online Library. Click here to view.
942			_2ddc _cER