| 000 -LEADER |
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| fixed length control field |
10745cam a2200409 i 4500 |
| 005 - DATE AND TIME OF LATEST TRANSACTION |
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| control field |
20250819083559.0 |
| 006 - FIXED-LENGTH DATA ELEMENTS--ADDITIONAL MATERIAL CHARACTERISTICS--GENERAL INFORMATION |
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| fixed length control field |
m o d |
| 007 - PHYSICAL DESCRIPTION FIXED FIELD--GENERAL INFORMATION |
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| fixed length control field |
cr cnu---unuuu |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
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| fixed length control field |
250819s2023 nyum o u000 0 eng d |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
|---|
| International Standard Book Number |
9781119010135 |
| Qualifying information |
hardcover |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
|---|
| International Standard Book Number |
9781119693376 |
| Qualifying information |
electronic book |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
|---|
| International Standard Book Number |
1119693373 |
| Qualifying information |
electronic book |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
|---|
| International Standard Book Number |
9781119693383 |
| Qualifying information |
electronic book |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
|---|
| International Standard Book Number |
1119693381 |
| Qualifying information |
electronic book |
| 035 ## - SYSTEM CONTROL NUMBER |
|---|
| System control number |
(OCoLC)1391432707 |
| 041 ## - LANGUAGE CODE |
|---|
| Language code of text/sound track or separate title |
eng |
| 050 #4 - LIBRARY OF CONGRESS CALL NUMBER |
|---|
| Classification number |
QD51 |
| Item number |
.A44 2023 |
| 082 04 - DEWEY DECIMAL CLASSIFICATION NUMBER |
|---|
| Classification number |
542.028/9 |
| Edition number |
23/eng/20230906 |
| 110 2# - MAIN ENTRY--CORPORATE NAME |
|---|
| Corporate name or jurisdiction name as entry element |
American Institute of Chemical Engineers. |
| Subordinate unit |
Center for Chemical Process Safety, |
| Authority record control number |
https://id.loc.gov/authorities/names/n85267114 |
| Relator term |
author. |
| 245 10 - TITLE STATEMENT |
|---|
| Title |
Handbook for process safety in laboratories and pilot plants : |
| Remainder of title |
a risk-based approach / |
| Statement of responsibility, etc |
Center for Chemical Process Safety, American Institute of Chemical Engineers. |
| 264 #1 - PUBLICATION, DISTRIBUTION, ETC. (IMPRINT) |
|---|
| Place of publication, distribution, etc |
New York, NY ; |
| Name of publisher, distributor, etc |
American Institute of Chemical Engineers ; |
| Place of publication, distribution, etc |
Hoboken, New Jersey : |
| Name of publisher, distributor, etc |
John Wiley & Sons, Inc., |
| Date of publication, distribution, etc |
[2023] |
| 300 ## - PHYSICAL DESCRIPTION |
|---|
| Extent |
1 online resource. |
| 336 ## - CONTENT TYPE |
|---|
| Content type term |
text |
| Content type code |
txt |
| Source |
rdacontent. |
| 337 ## - MEDIA TYPE |
|---|
| Media type term |
computer |
| Media type code |
c |
| Source |
rdamedia. |
| 338 ## - CARRIER TYPE |
|---|
| Carrier type term |
online resource |
| Carrier type code |
cr |
| Source |
rdacarrier. |
| 340 ## - PHYSICAL MEDIUM |
|---|
| Source |
rdacc |
| Authority record control number or standard number |
http://rdaregistry.info/termList/RDAColourContent/1003. |
| 490 1# - SERIES STATEMENT |
|---|
| Series statement |
CCPS handbook. |
| 505 0# - CONTENTS |
|---|
| Formatted contents note |
Table of Contents<br/>List of Figures x<br/><br/>List of Tables xi<br/><br/>Abbreviations and Acronyms xii<br/><br/>Glossary xv<br/><br/>Acknowledgments xxii<br/><br/>Dedication xxiv<br/><br/>Online Materials Accompanying this Handbook xxv<br/><br/>Preface xxvii<br/><br/>Part 1 – Introduction and Overview 1<br/><br/>1 Purpose and Scope 3<br/><br/>1.1 Purpose 3<br/><br/>1.2 Scope of Book and Target Audience 4<br/><br/>1.3 Terms for Laboratories and Pilot Plants 5<br/><br/>1.4 Distinctions between Laboratories and Pilot Plants 7<br/><br/>1.5 Organization of This Handbook 8<br/><br/>2 Managing Risk to Prevent Incidents 13<br/><br/>2.1 Some LAPP Characteristics 13<br/><br/>2.2 Safety in Laboratories and Pilot Plants 24<br/><br/>2.3 Where to Start with a Risk-based Approach in the LAPP 25<br/><br/>2.4 Gain Leadership Support to Implement Risk Based Process Safety 29<br/><br/>2.5 Laboratory Safety Management System Considerations 29<br/><br/>2.6 Resources for Risk Based Process Safety Management System 31<br/><br/>3 Leaks and Spills in the LAPP 35<br/><br/>3.1 Leaks of Hazardous Materials 35<br/><br/>3.2 Spills of Hazardous Materials 38<br/><br/>Part 2 – Committing to Process Safety 39<br/><br/>4 LAPP Risk Management Concepts 41<br/><br/>4.1 Occupational Safety and Process Safety 41<br/><br/>4.2 Hierarchy of Controls 41<br/><br/>4.3 Inherently Safer Design (ISD) 42<br/><br/>4.4 Basic Risk Concepts 44<br/><br/>4.5 A Risk Management Program 47<br/><br/>4.6 Anatomy of an Incident 48<br/><br/>4.7 Preventive and Mitigative Safeguards 49<br/><br/>4.8 Applying a Risk-Based Approach in a LAPP 51<br/><br/>5 Process Safety Culture in the LAPP 55<br/><br/>5.1 RBPS Element 1: Process Safety Culture 55<br/><br/>5.2 Leaders’ Responsibilities for Positive Safety Culture 58<br/><br/>5.3 Resources and Examples for Process Safety Culture 59<br/><br/>6 Standards for the LAPP 63<br/><br/>6.1 RBPS Element 2: Compliance with Standards 63<br/><br/>6.2 Risk Management Focus 65<br/><br/>6.3 Different Codes and Standards When Scaling Up from Laboratory to Pilot Plant 65<br/><br/>6.4 Jurisdictional Requirements 67<br/><br/>6.5 Resources for Compliance with Standards 67<br/><br/>7 Process Safety Competency and Training in the LAPP 69<br/><br/>7.1 RBPS Element 3: Process Safety Competency 69<br/><br/>7.2 RBPS Element 12: Training and Performance Assurance 72<br/><br/>8 Workforce Involvement and Stakeholder Outreach in the LAPP 79<br/><br/>8.1 RBPS Element 4: Workforce Involvement 79<br/><br/>8.2 RBPS Element 5: Stakeholder Outreach 82<br/><br/>Part 3 – Understanding Hazards and Risks 83<br/><br/>9 Process Safety Knowledge Management in the LAPP 85<br/><br/>9.1 RBPS Element 6: Process Knowledge Management 85<br/><br/>9.2 Overview of Information and Data Needs 86<br/><br/>9.3 Sources of Information and Data 89<br/><br/>9.4 Process Safety Information during Scale-up 92<br/><br/>10 Types of Hazards 95<br/><br/>10.1 Reactive Chemistry Hazards 95<br/><br/>10.2 Toxicity Hazards 115<br/><br/>10.3 Flammability and Combustibility Hazards 121<br/><br/>10.4 Temperature Hazards 137<br/><br/>10.5 Overpressure Hazards 140<br/><br/>10.6 Other Common LAPP Hazards 142<br/><br/>Table of Contents vii ix<br/><br/>11 Hazard Identification and Risk Analysis (HIRA) in the LAPP 153<br/><br/>11.1 RBPS Element 7: Hazard Identification and Risk Analysis 153<br/><br/>11.2 HIRA Team Members 156<br/><br/>11.3 HIRA Approaches Used in LAPPs 156<br/><br/>11.4 Qualitative versus Quantitative Analysis of Risks in LAPPs 165<br/><br/>11.5 ACS Hazard Analysis Tools 168<br/><br/>11.6 Evaluating the Effort Level for HIRAs 168<br/><br/>11.7 Determining the Extent of the HIRAs 169<br/><br/>Part 4 – Managing Risk: Engineered Controls 171<br/><br/>12 Spill and Leak Protection 173<br/><br/>12.1 Containment 173<br/><br/>12.2 Flexible hose and tubing 173<br/><br/>13 Fire and Over-Temperature Protection 175<br/><br/>13.1 Fire Prevention 175<br/><br/>13.2 Fire Mitigation 183<br/><br/>13.3 Over-Temperature Protection 185<br/><br/>14 Overpressure Prevention and Protection 191<br/><br/>14.1 Pressure Protection for Equipment 191<br/><br/>14.2 Pressure and Vacuum Relief for Atmospheric Pressure Vessels 196<br/><br/>14.3 Process Conditions/Situations to Consider in Pressure Relief Device Design 197<br/><br/>14.4 Blast Containment Cells and Pressure Relief for Building Areas 198<br/><br/>14.5 Venting Location and Downstream Treatment of Material Vented 201<br/><br/>15 Ventilation Controls 203<br/><br/>15.1 Ventilation Systems 203<br/><br/>15.2 Laboratory Chemical Fume Hoods 205<br/><br/>15.3 Pilot Plant Ventilation 207<br/><br/>15.4 Permanent Total Enclosures for Containment in the LAPP 207<br/><br/>16 Automated Shut-down Systems 209<br/><br/>16.1 Selection and Design Based on Hazard Identification and Risk Analysis 209<br/><br/>16.2 Basic Control Systems and Safety Shut-down Systems 209<br/><br/>16.3 Independent Automated Safety Shut-down Systems 210<br/><br/>16.4 Fail-Safe Design Considerations 212<br/><br/>16.5 Important Design Features for Control Systems 212<br/><br/>16.6 Control of Changes and Maintenance for Engineered Safeguards 214<br/><br/>16.7 Additional References 215<br/><br/>17 Engineered Controls for Common Hazards 217<br/><br/>17.1 Cryogenic Fluids and Compressed Gases 217<br/><br/>17.2 Cryogenic Fluids and Compressed Gas Cylinders 218<br/><br/>17.3 Glass Equipment 228<br/><br/>17.4 Gloveboxes 228<br/><br/>Part 5 – Managing Risk: Administrative Controls 235<br/><br/>18 Administrative Fire and Explosion Safeguards 237<br/><br/>18.1 Standards and Guidance for Fire Prevention 237<br/><br/>18.2 Ignition Source Control: Procedures 237<br/><br/>18.3 Manual Fire Suppression 238<br/><br/>19 Administrative Safeguards for Hazards in LAPPs 239<br/><br/>19.1 Good Practices for Compressed Gas and Cryogenic Cylinders 239<br/><br/>19.2 Regulations and Standards for Compressed Gases and Cryogenic Fluids 239<br/><br/>19.3 Procedures and Best Practices for Compressed Gases 241<br/><br/>19.4 Good Practices for Storage, Movement, and Use of Cryogenic Fluids 248<br/><br/>19.5 Good Practices For Handling Glass 251<br/><br/>19.6 Administrative Controls for Reactive Hazards 251<br/><br/>Part 6 – Managing Risk: RBPS Management Systems 253<br/><br/>20 Operating Procedures and Conduct of Operations in the LAPP 255<br/><br/>20.1 RBPS Element 8: LAPP Operating Procedures 255<br/><br/>20.2 RBPS Element 15: Conduct of Operations 260<br/><br/>21 Safe Work Practices and Contractor Management in the LAPP 263<br/><br/>21.1 RBPS Element 9: Safe Work Practices 263<br/><br/>21.2 RBPS Element 11: Contractor Management 266<br/><br/>22 Asset Integrity and Reliability in the LAPP 269<br/><br/>22.1 RBPS Element 10: Asset Integrity and Reliability 269<br/><br/>22.2 A Management Approach for Assuring Asset Integrity and Reliability 270<br/><br/>22.3 Examples of Asset Integrity and Reliability Management System Failures 271<br/><br/>22.4 Glass Equipment—Asset Integrity and Reliability Challenge for LAPPs 274<br/><br/>23 Management of Change (MOC) and Operational Readiness in the LAPP 277<br/><br/>23.1 RBPS Element 13: Management of Change 277<br/><br/>23.2 RBPS Element 14: Operational Readiness 281<br/><br/>Table of Contents ix xi<br/><br/>24 Emergency Management in the LAPP 283<br/><br/>24.1 RBPS Element 16: Emergency Management 283<br/><br/>24.2 Emergency Planning 283<br/><br/>24.3 Implementing an Emergency Management Plan 284<br/><br/>24.4 Emergency Equipment 285<br/><br/>24.5 Training and Drills 285<br/><br/>24.6 Deficiencies in Emergency Planning and Response in LAPP Cases 286<br/><br/>24.7 Controlling Unattended Experimental Work and Working Alone in LAPPs 288<br/><br/>Part 7 – Learning from Experience 291<br/><br/>25 Investigating Incidents 293<br/><br/>25.1 Incident Terminology 293<br/><br/>25.2 RBPS Element 17: Incident Investigation 294<br/><br/>25.3 Steps of an Incident Investigation 295<br/><br/>25.4 Ensure Lessons Are Learned and Remembered 298<br/><br/>25.5 Learn from Experience of Others 298<br/><br/>26 Metrics, Auditing, and Management Review in the LAPP 299<br/><br/>26.1 RBPS Element 18: Measurement and Metrics 299<br/><br/>26.2 RBPS Element 19: Auditing 300<br/><br/>26.3 RBPS Element 20: Management Review and Continuous Improvement 302<br/><br/>Part 8 – Conclusion 305<br/><br/>References 307<br/><br/>Appendix A Cases 323<br/><br/>Appendix B Examples 453<br/><br/>Appendix C Control Banding Strategies 501<br/><br/>Appendix D Glass Equipment Design 517<br/><br/>Index 525 |
| 520 ## - SUMMARY, ETC. |
|---|
| Summary, etc |
In Handbook for Process Safety in Laboratories and Pilot Plants: A Risk-based Approach, the Center for Chemical Process Safety delivers a comprehensive and authoritative presentation of process safety procedures and methods for use in laboratories and pilot plants (LAPPs). Of the four broad hazard categories - chemical, physical, biological, and ionizing radiation - this book focuses on the two most common: chemical and physical hazards. It addresses the storage and handling of the hazardous materials associated with activities commonly performed in LAPPs and presents many of the physical and chemical analytical techniques used to verify and validate the efficacy of safety management systems. This book will present tools and techniques for effectively managing the risks in any laboratory or pilot plant using engineered and administrative controls, as well as the CCPS Risk Based Process Safety (RBPS) Management Systems. |
| 545 0# - BIOGRAPHICAL OR HISTORICAL DATA |
|---|
| Biographical or historical note |
About the Author<br/>Since 1985, the Center for Chemical Process Safety (CCPS) has been the global leader in developing and disseminating information on process safety management and technology. CCPS, an industry technology alliance of the American Institute of Chemical Engineers (AIChE), has published over 100 books in its process safety guidelines and process safety concepts series, and over 100 training modules through its Safety in Chemical Engineering Education (SACHE) series. |
| 650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
|---|
| Topical term or geographic name as entry element |
Chemical laboratories |
| General subdivision |
Safety measures. |
| Authority record control number |
https://id.loc.gov/authorities/subjects/sh2009118821. |
| 655 #4 - INDEX TERM--GENRE/FORM |
|---|
| Genre/form data or focus term |
Electronic books. |
| 830 #0 - SERIES ADDED ENTRY--UNIFORM TITLE |
|---|
| Uniform title |
CCPS handbook. |
| 856 40 - ELECTRONIC LOCATION AND ACCESS |
|---|
| Uniform Resource Identifier |
https://onlinelibrary.wiley.com/doi/book/10.1002/9781119693383 |
| Link text |
Full text is available at Wiley Online Library Click here to view |
| 942 ## - ADDED ENTRY ELEMENTS |
|---|
| Source of classification or shelving scheme |
|
| Item type |
EBOOK |